2KQD

First PBZ domain of human APLF protein in complex with ribofuranosyladenosine

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	800
2	Bruker	DMX	Bruker DMX	600
3	Bruker	DRX	Bruker DRX	500

Experiment

experiment id	conditions id	solution id	Experiment type
1	3	1	2D 1H-15N HSQC
10	2	2	3D 1H-13C NOESY
11	2	2	2D 1H-1H TOCSY
2	1	2	2D 1H-13C HSQC full-width
3	1	2	2D 1H-1H NOESY
4	1	2	2D 1H-1H NOESY filtered
5	1	2	3D 1H-13C NOESY
6	1	2	2D 1H-1H TOCSY
7	2	2	2D 1H-13C HSQC full-width
8	2	2	2D 1H-1H NOESY
9	2	2	2D 1H-1H NOESY filtered

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6	ambient	278
2	6	ambient	286
3	6	ambient	300

Conformers

Conformers Calculated Total Number	50
Conformers Submitted Total Number	10