2JVE

Solution structure of the extracellular domain of Prod1, a protein implicated in proximodistal identity during amphibian limb regeneration

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Varian	INOVA	Varian INOVA	800
2	Varian	INOVA	Varian INOVA	600
3	Varian	INOVA	Varian INOVA	600
4	Varian	UNITYPLUS	Varian UnityPlus	500

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D HN(CO)CA
11	1	2	3D HN(CA)CO
12	1	2	3D HA(CA)NH
13	1	2	3D HN(CACO)NH
14	1	3	3D HCCH-TOCSY
15	1	3	3D HCCH-COSY
16	1	1	3D 1H-15N TOCSY
2	1	3	2D 1H-13C HSQC
3	1	1	3D 1H-15N NOESY
4	1	3	3D 1H-13C NOESY
5	1	3	3D 1H-13C aromatic NOESY
6	1	2	3D CBCA(CO)NH
7	1	2	3D HNCO
8	1	2	3D HNCA
9	1	2	3D HNCACB

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.5	ambient	298

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	20