2JLY
Dengue virus 4 NS3 helicase in complex with ssRNA and ADP-Phosphate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 131.748, 105.591, 72.671 |
| Unit cell angles | 90.00, 117.68, 90.00 |
Refinement procedure
| Resolution | 19.990 - 2.400 |
| R-factor | 0.20194 |
| Rwork | 0.199 |
| R-free | 0.25494 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2jlu |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.134 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.800 | 2.500 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.140 | 0.720 |
| Number of reflections | 188211 | |
| <I/σ(I)> | 13.8 | 1.7 |
| Completeness [%] | 99.6 | 97.5 |
| Redundancy | 5.5 | 5.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
