2JJE

Crystal structure of T330S mutant of Rv3290c from M. tuberculosis

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	298
Spacegroup name	P 31 2 1
Unit cell lengths	103.244, 103.244, 98.195
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	89.440 - 2.200
R-factor	0.159
Rwork	0.158
R-free	0.18700
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.009
RMSD bond angle	1.216
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall
Low resolution limit [Å]	21.520
High resolution limit [Å]	2.200
Rmerge	0.100
Number of reflections	30104
<I/σ(I)>	13.3
Completeness [%]	97.4
Redundancy	5.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1