2JHM
Structure of globular heads of M-ficolin at neutral pH
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-2 |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-07-01 |
| Detector | ADSC CCD |
| Spacegroup name | H 3 |
| Unit cell lengths | 73.709, 73.709, 124.605 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 56.800 - 1.520 |
| R-factor | 0.184 |
| Rwork | 0.182 |
| R-free | 0.20700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2j3g |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.187 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 56.800 |
| High resolution limit [Å] | 1.520 |
| Rmerge | 0.070 |
| Number of reflections | 36615 |
| <I/σ(I)> | 11.3 |
| Completeness [%] | 94.3 |
| Redundancy | 2.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | pH 7 |
