2JHJ
3-methyladenine dna-glycosylase from Archaeoglobus fulgidus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-01-13 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 69.890, 48.850, 104.460 |
Unit cell angles | 90.00, 106.07, 90.00 |
Refinement procedure
Resolution | 12.000 - 1.900 |
R-factor | 0.184 |
Rwork | 0.181 |
R-free | 0.23900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jhn |
RMSD bond length | 0.015 |
RMSD bond angle | 1.366 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.950 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.070 | 0.430 |
Number of reflections | 53742 | |
<I/σ(I)> | 11.4 | 2.5 |
Completeness [%] | 99.9 | 100 |
Redundancy | 2.9 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1M BICINE, PH9.0 10% W/V PEG20000 2% V/V DIOXANE |