2JH5
Human Thrombin Hirugen Inhibitor complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ENRAF-NONIUS FR591 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-05-20 |
| Detector | NONIUS |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 70.363, 71.478, 72.106 |
| Unit cell angles | 90.00, 100.62, 90.00 |
Refinement procedure
| Resolution | 19.710 - 2.500 |
| R-factor | 0.188 |
| Rwork | 0.185 |
| R-free | 0.23100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.629 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.3.0006) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.710 | 2.580 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmerge | 0.040 | 0.330 |
| Number of reflections | 11571 | |
| Completeness [%] | 98.0 | |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.8 | PH 6.80 |
