2JH5
Human Thrombin Hirugen Inhibitor complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR591 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-05-20 |
Detector | NONIUS |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 70.363, 71.478, 72.106 |
Unit cell angles | 90.00, 100.62, 90.00 |
Refinement procedure
Resolution | 19.710 - 2.500 |
R-factor | 0.188 |
Rwork | 0.185 |
R-free | 0.23100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.629 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.3.0006) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.710 | 2.580 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.040 | 0.330 |
Number of reflections | 11571 | |
Completeness [%] | 98.0 | |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.8 | PH 6.80 |