2JB5
Fab fragment in complex with small molecule hapten, crystal form-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-06-30 |
Detector | MARRESEARCH |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 71.949, 98.480, 153.782 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.700 - 2.800 |
Rwork | 0.211 |
R-free | 0.27150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1vge |
RMSD bond length | 0.007 |
RMSD bond angle | 1.400 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | CNX (2005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.700 | 2.850 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.100 | 0.550 |
Number of reflections | 13432 | |
<I/σ(I)> | 17.1 | 2.2 |
Completeness [%] | 97.6 | 79.8 |
Redundancy | 5.5 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 | 2.3M AMMONIUM SULPHATE, 5% PEG400, 0.1M SODIUM CITRATE PH 4.0, FOR CRYO BUFFER ADITIONAL 15% GLYCEROL |