2J67
The TIR domain of human Toll-Like Receptor 10 (TLR10)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-08-22 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 66.200, 43.300, 71.300 |
Unit cell angles | 90.00, 101.00, 90.00 |
Refinement procedure
Resolution | 23.430 - 2.200 |
R-factor | 0.216 |
Rwork | 0.214 |
R-free | 0.26600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1fyv |
RMSD bond length | 0.015 |
RMSD bond angle | 1.524 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 23.000 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.060 | 0.400 |
Number of reflections | 19993 | |
<I/σ(I)> | 13.8 | 3.5 |
Completeness [%] | 97.6 | 92 |
Redundancy | 3.8 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.2 M NASCN, 11% PEG 3350 |