2J0G
L-ficolin complexed to N-acetyl-mannosamine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-04-21 |
Detector | ADSC CCD |
Spacegroup name | P 32 |
Unit cell lengths | 96.940, 96.940, 139.470 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.850 |
R-factor | 0.196 |
Rwork | 0.193 |
R-free | 0.24800 |
Structure solution method | OTHER |
RMSD bond length | 0.011 |
RMSD bond angle | 1.394 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.800 |
Rmerge | 0.080 |
Number of reflections | 33923 |
<I/σ(I)> | 11.6 |
Completeness [%] | 97.6 |
Redundancy | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |