2IZU
Structure of casein kinase gamma 3 in complex with inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-04-23 |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 56.903, 56.903, 222.529 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 27.570 - 1.850 |
R-factor | 0.157 |
Rwork | 0.155 |
R-free | 0.19900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2chl |
RMSD bond length | 0.011 |
RMSD bond angle | 1.233 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.500 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.060 | 0.390 |
Number of reflections | 32225 | |
<I/σ(I)> | 17.7 | 1.6 |
Completeness [%] | 80.7 | 24.7 |
Redundancy | 4.5 | 1.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 20% PEG3350, 0.20 M NAFORMATE |