2IYP
product rup
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2004-05-17 |
| Detector | RIGAKU IMAGE PLATE |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 71.062, 105.061, 240.484 |
| Unit cell angles | 90.00, 98.26, 90.00 |
Refinement procedure
| Resolution | 29.810 - 2.790 |
| R-factor | 0.182 |
| Rwork | 0.179 |
| R-free | 0.25500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.307 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.900 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rmerge | 0.080 | 0.250 |
| Number of reflections | 39483 | |
| <I/σ(I)> | 6.5 | 3 |
| Completeness [%] | 90.7 | 81.9 |
| Redundancy | 1.8 | 1.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.2 | 25% PEG 3350, 0.1M SODIUM CACODYLATE, 300MM AMMONIUM ACETATE, pH 7.20 |
