2IXI

RmlC P aeruginosa with dTDP-xylose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SRS BEAMLINE PX9.6
Synchrotron site	SRS
Beamline	PX9.6
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	P 21 21 2
Unit cell lengths	64.785, 148.065, 45.434
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	74.540 - 1.800
R-factor	0.188
Rwork	0.186
R-free	0.23700
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2ixj
RMSD bond length	0.009
RMSD bond angle	1.609
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	REFMAC (5.2.0007)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.000	1.900
High resolution limit [Å]	1.800	1.800
Rmerge	0.100	0.350
Number of reflections	35190
<I/σ(I)>	5.2	2
Completeness [%]	80.0	67
Redundancy	3	3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1