2IBZ
Yeast Cytochrome BC1 Complex with Stigmatellin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-3 |
Synchrotron site | ESRF |
Beamline | ID14-3 |
Temperature [K] | 277 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 214.473, 163.921, 147.276 |
Unit cell angles | 90.00, 117.50, 90.00 |
Refinement procedure
Resolution | 14.960 - 2.300 |
Rwork | 0.222 |
R-free | 0.25600 |
Structure solution method | MIR |
RMSD bond length | 0.008 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 14.960 | 2.440 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.390 | |
Number of reflections | 168517 | |
<I/σ(I)> | 12.4 | 1.2 |
Completeness [%] | 84.6 | 72.9 |
Redundancy | 6.3 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | precipitant PEG4000, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K |