2I6A
Human Adenosine Kinase in Complex With 5'-Deoxy-5-Iodotubercidin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 110 |
| Wavelength(s) | 1.00000 |
| Spacegroup name | P 1 |
| Unit cell lengths | 61.850, 66.930, 87.140 |
| Unit cell angles | 97.76, 103.70, 89.95 |
Refinement procedure
| Resolution | 50.000 - 2.200 |
| Rwork | 0.181 |
| R-free | 0.27100 |
| Structure solution method | MIR |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | DM |
| Refinement software | BUSTER |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.200 |
| Number of reflections | 35353 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 298 | PEG 4000, 0.1 M MgCl2, pH 7.2, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
