2HKH
Crystal structure of the Fab M75
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR591 |
Temperature [K] | 150 |
Detector technology | IMAGE PLATE |
Collection date | 2001-03-10 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | P 1 |
Unit cell lengths | 40.982, 43.154, 57.370 |
Unit cell angles | 85.30, 88.45, 84.29 |
Refinement procedure
Resolution | 20.460 - 2.100 |
R-factor | 0.22394 |
Rwork | 0.219 |
R-free | 0.27292 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1nbv |
RMSD bond length | 0.011 |
RMSD bond angle | 1.547 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | EPMR |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.069 | 0.304 |
Number of reflections | 57110 | |
<I/σ(I)> | 6.5 | |
Completeness [%] | 90.7 | 68.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | 15% PEG 4000, 100 mM Tris, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |