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2GSE

Crystal Structure of Human Dihydropyrimidinease-like 2

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-2
Synchrotron siteESRF
BeamlineID14-2
Temperature [K]173
Detector technologyCCD
Collection date2006-02-12
DetectorADSC QUANTUM 4
Wavelength(s)0.933
Spacegroup nameP 1 21 1
Unit cell lengths86.400, 126.100, 102.900
Unit cell angles90.00, 113.00, 90.00
Refinement procedure
Resolution29.310 - 2.400
R-factor0.173
Rwork0.169
R-free0.24500
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.015
RMSD bond angle1.567
Data scaling softwareXDS
Phasing softwareMOLREP
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.600
High resolution limit [Å]2.4002.400
Rmerge0.1430.430
Number of reflections79142
<I/σ(I)>9.63.36
Completeness [%]99.799.7
Redundancy4.34.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.529518% PEG 10k, 0.1M Tris, 0.2M CaCl, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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