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2GJ4

Structure of rabbit muscle glycogen phosphorylase in complex with ligand

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSRS BEAMLINE PX9.6
Synchrotron siteSRS
BeamlinePX9.6
Temperature [K]100
Detector technologyCCD
Collection date2001-10-24
DetectorADSC QUANTUM 4
Wavelength(s)0.87
Spacegroup nameP 43 21 2
Unit cell lengths128.128, 128.128, 116.346
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution48.800 - 1.600
R-factor0.1889
Rwork0.187
R-free0.22616
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)In house model
RMSD bond length0.009
RMSD bond angle1.184
Data reduction softwareMOSFLM
Phasing softwareAMoRE
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]48.8001.690
High resolution limit [Å]1.6001.600
Rmerge0.0590.466
Number of reflections94754
<I/σ(I)>121.5
Completeness [%]74.574.5
Redundancy3.31.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.72891.1mM IMP, 1.1mM Spermine, 0mM BES, 2.9mM DTT, 0.1mM EDTA, pH 6.7, VAPOR DIFFUSION, SITTING DROP, temperature 289K

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