2GBC
Native DPP-IV (CD26) from Rat
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 3 |
Unit cell lengths | 208.152, 208.152, 208.152 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.800 |
Rwork | 0.229 |
R-free | 0.25800 |
Structure solution method | MIR |
RMSD bond length | 0.008 |
RMSD bond angle | 1.470 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 6.030 | 2.800 |
Rmerge | 0.089 | 0.058 | 0.468 |
Number of reflections | 73192 | 7617 | 7157 |
<I/σ(I)> | 12.9 | ||
Completeness [%] | 98.7 | ||
Redundancy | 5.3 | 5.9 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5 | 290 | pH 5, VAPOR DIFFUSION, temperature 290K |