2GA2

h-MetAP2 complexed with A193400

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	110
Wavelength(s)	1.54
Spacegroup name	C 2 2 21
Unit cell lengths	89.731, 98.793, 101.213
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.790 - 1.950
R-factor	0.2
Rwork	0.202
R-free	0.25100
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.300
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNX (2002)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.020
High resolution limit [Å]	1.950	1.950
Number of reflections	28808
<I/σ(I)>	22	3
Completeness [%]	87.1	87.6
Redundancy	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1