2G73
Y104F mutant type 1 IPP isomerase complex with EIPP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR591 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2005-06-30 |
Detector | MARRESEARCH |
Wavelength(s) | 1.54179 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 68.935, 71.477, 91.955 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.970 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1hx3 |
RMSD bond length | 0.029 |
RMSD bond angle | 0.023 |
Phasing software | SHELX |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 | 2.030 |
High resolution limit [Å] | 1.970 | 1.970 |
Rmerge | 0.055 | 0.250 |
Number of reflections | 28124 | |
<I/σ(I)> | 6.2 | |
Completeness [%] | 99.1 | 92.4 |
Redundancy | 6.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 295 | PEG 2000 mme, MANGANESE AND MAGNESIUM CHLORIDE, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K |