2FVV
Human Diphosphoinositol polyphosphate phosphohydrolase 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-12-27 |
Detector | Bruker Platinum 135 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.653, 59.900, 61.735 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.250 |
R-factor | 0.171 |
Rwork | 0.171 |
R-free | 0.22200 |
Structure solution method | SAD |
RMSD bond length | 0.017 |
RMSD bond angle | 0.037 |
Data reduction software | PROTEUM PLUS |
Data scaling software | SADABS |
Phasing software | SHELXD |
Refinement software | SHELX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.440 | 1.340 |
High resolution limit [Å] | 1.250 | 1.250 |
Rmerge | 0.081 | 0.276 |
Number of reflections | 45852 | |
<I/σ(I)> | 23.93 | 2.74 |
Completeness [%] | 90.5 | 58.1 |
Redundancy | 8.88 | 1.55 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 277 | 30% PEG8000, 0.2M Lithium sulphate, 0.1M SODIUM ACETATE, pH 4.5, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 277 | 30% PEG8000, 0.2M Lithium sulphate, 0.1M SODIUM ACETATE, pH 4.5, VAPOR DIFFUSION, SITTING DROP, temperature 277K |