2FS4
Ketopiperazine-Based Renin Inhibitors: Optimization of the C ring
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Spacegroup name | P 21 3 |
Unit cell lengths | 141.917, 141.917, 141.917 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 2.200 |
R-factor | 0.243 |
Rwork | 0.243 |
R-free | 0.28400 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 25.000 |
High resolution limit [Å] | 2.200 |
Number of reflections | 47471 |
Completeness [%] | 1.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |