2FLU
Crystal Structure of the Kelch-Neh2 Complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 110 |
Detector technology | CCD |
Wavelength(s) | 1.23983 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 76.757, 92.069, 46.314 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.000 - 1.500 |
R-factor | 0.18048 |
Rwork | 0.179 |
R-free | 0.19867 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1u6d |
RMSD bond length | 0.009 |
RMSD bond angle | 1.211 |
Data scaling software | d*TREK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.400 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.077 | 0.456 |
Number of reflections | 50551 | |
<I/σ(I)> | 11.1 | 2.1 |
Completeness [%] | 94.7 | 64.6 |
Redundancy | 6.3 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8.5 | 277 | 100 mM TrisHCl 200 mM MgCl2 30% PEG 4000, pH 8.5, VAPOR DIFFUSION, temperature 277K |