2FJ9
High resolution crystal structure of the unliganded human ACBP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2000-08-02 |
Detector | MARRESEARCH |
Wavelength(s) | 0.91 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 43.824, 43.824, 177.247 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 14.830 - 1.600 |
R-factor | 0.196 |
Rwork | 0.196 |
R-free | 0.22900 |
Structure solution method | SAD |
RMSD bond length | 0.023 |
RMSD bond angle | 2.200 |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.620 |
High resolution limit [Å] | 1.560 | 1.560 |
Number of reflections | 14797 | |
<I/σ(I)> | 31.9 | |
Completeness [%] | 95.9 | 98.5 |
Redundancy | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 25% PEG-MME 550, 100mM MES, pH 6.5, 10mM ZnSO4, 3% 1-propanol, VAPOR DIFFUSION, HANGING DROP, temperature 298K |