2FCI
Structural basis for the requirement of two phosphotyrosines in signaling mediated by Syk tyrosine kinase
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | DRX | 500 | |
| 2 | Varian | INOVA | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | CBCA(CO)NH |
| 10 | 1 | 1 | Double x-filtered NOESY |
| 11 | 1 | 1 | Double x-filtered tocsy |
| 2 | 1 | 1 | HNCACB |
| 3 | 1 | 1 | HCCH-TOCSY |
| 4 | 1 | 1 | 15N HSQC-TOCSY |
| 5 | 1 | 1 | 15N HSQC-NOESY |
| 6 | 1 | 1 | C(CO)NH |
| 7 | 1 | 1 | HC(CO)NH |
| 8 | 1 | 1 | HNCA |
| 9 | 1 | 1 | Single x-fileted NOESY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6 | 1 | 278 |
Conformers
| Conformers Calculated Total Number | 50 |
| Conformers Submitted Total Number | 16 |
