2F4U
Asite RNA + designer antibiotic
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 100 |
Collection date | 2002-06-01 |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 33.100, 46.460, 89.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.230 - 2.600 |
R-factor | 0.299 |
Rwork | 0.250 |
R-free | 0.29900 |
Structure solution method | MOLECULAR REPLACEMENT |
Data scaling software | d*TREK |
Refinement software | CNS |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 23.230 | 23.230 | 2.690 |
High resolution limit [Å] | 2.600 | 5.580 | 2.600 |
Rmerge | 0.092 | 0.423 | |
Number of reflections | 4451 | ||
<I/σ(I)> | 5.8 | 1.6 | |
Completeness [%] | 97.6 | 93.2 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |