2EXE
Crystal structure of the phosphorylated CLK3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-09-03 |
Detector | MARRESEARCH |
Wavelength(s) | 0.97640 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 62.180, 110.998, 161.544 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.820 - 2.350 |
R-factor | 0.22653 |
Rwork | 0.225 |
R-free | 0.26028 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1z57 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.235 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.820 | |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.050 | 0.343 |
Number of reflections | 23665 | |
<I/σ(I)> | 13.59 | |
Completeness [%] | 99.6 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | 1.8M (NH4)3(cit), pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K |