2D4K
Monoclinic hen egg-white lysozyme crystallized at 313K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | MACSCIENCE |
Temperature [K] | 290 |
Detector technology | CCD |
Collection date | 2002-05-29 |
Detector | BRUKER SMART 6000 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 27.217, 63.484, 59.189 |
Unit cell angles | 90.00, 92.93, 90.00 |
Refinement procedure
Resolution | 19.700 - 1.150 |
R-factor | 0.133 |
Rwork | 0.132 |
R-free | 0.16400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1lys |
RMSD bond length | 0.015 |
RMSD bond angle | 0.032 |
Data reduction software | SaintPlus |
Data scaling software | SAINTPLUS |
Phasing software | X-PLOR |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.700 | 1.170 |
High resolution limit [Å] | 1.150 | 1.150 |
Rmerge | 0.119 | 0.336 |
Number of reflections | 67029 | |
Completeness [%] | 93.9 | 62.2 |
Redundancy | 4.14 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | batch method | 7.6 | 313 | 2% protein, 10% sodium chloride, 5% 1-propanol, pH 7.6, batch method, temperature 313K |