2D3M
Pentaketide chromone synthase complexed with coenzyme A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL24XU |
Synchrotron site | SPring-8 |
Beamline | BL24XU |
Detector technology | IMAGE PLATE |
Collection date | 2004-10-07 |
Detector | RIGAKU RAXIS V |
Wavelength(s) | 0.82656 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 73.150, 88.400, 70.040 |
Unit cell angles | 90.00, 95.58, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.600 |
Rwork | 0.198 |
R-free | 0.20700 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.600 |
Number of reflections | 116521 |
Completeness [%] | 99.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |