2CF2

Architecture of mammalian fatty acid synthase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	CCD
Collection date	2005-04-16
Detector	MARRESEARCH
Spacegroup name	P 1 21 1
Unit cell lengths	96.100, 245.000, 134.100
Unit cell angles	90.00, 101.20, 90.00

Refinement procedure

Resolution	50.000 - 4.300
Structure solution method	MIRAS
Data reduction software	XDS
Data scaling software	XDS
Phasing software	SHARP

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	4.500
High resolution limit [Å]	4.300	4.300
Rmerge	0.120	0.410
Number of reflections	41085
<I/σ(I)>	10	4
Completeness [%]	99.1	99.5
Redundancy	4.2	4.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1