2CDH

ARCHITECTURE OF THE THERMOMYCES LANUGINOSUS FUNGAL FATTY ACID SYNTHASE AT 5 ANGSTROM RESOLUTION.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 1 21 1
Unit cell lengths	217.000, 415.000, 222.000
Unit cell angles	90.00, 111.50, 90.00

Refinement procedure

Resolution	500.000 - 4.200
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	PDB ENTRIES 1S9C 1dd8 1edo 1GOX AND 1NM2
Data reduction software	XDS
Data scaling software	XSCALE

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	500.000	4.500
High resolution limit [Å]	4.200	4.200
Rmerge	0.150	0.610
Number of reflections	261067
<I/σ(I)>	6.6	2.2
Completeness [%]	98.0	97.5
Redundancy	3.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1