2C3X

Structure of iodinated CBM25 from Bacillus halodurans amylase in complex with maltotetraose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113
Spacegroup name	P 43 21 2
Unit cell lengths	64.743, 64.743, 187.180
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	60.860 - 2.700
R-factor	0.215
Rwork	0.212
R-free	0.28300
Structure solution method	OTHER
RMSD bond length	0.014
RMSD bond angle	1.781
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.700
Rmerge	0.120
Number of reflections	11016
<I/σ(I)>	10.7
Completeness [%]	99.5
Redundancy	6.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1