2C3E

The bovine mitochondrial ADP-ATP carrier

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE BM30A
Synchrotron site	ESRF
Beamline	BM30A
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	C 2 2 21
Unit cell lengths	76.246, 110.752, 89.540
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.000 - 2.800
R-factor	0.2497
Rwork	0.250
R-free	0.28080
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1okc
RMSD bond length	0.009
RMSD bond angle	1.300
Data reduction software	DENZO
Data scaling software	CCP4
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	25.000	2.980
High resolution limit [Å]	2.800	2.800
Rmerge	0.110	0.560
Number of reflections	9435
<I/σ(I)>	4	1.1
Completeness [%]	99.9	99.9
Redundancy	16.7	6.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1