2C0C
Structure of the MGC45594 gene product
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-08-05 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 61.164, 82.137, 73.905 |
Unit cell angles | 90.00, 112.54, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.450 |
R-factor | 0.166 |
Rwork | 0.163 |
R-free | 0.21600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qor |
RMSD bond length | 0.018 |
RMSD bond angle | 1.764 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.500 | 1.550 |
High resolution limit [Å] | 1.450 | 1.450 |
Rmerge | 0.110 | 0.540 |
Number of reflections | 116573 | |
<I/σ(I)> | 11.24 | 2.27 |
Completeness [%] | 97.7 | 96.1 |
Redundancy | 4.89 | 3.18 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9.1 | 0.1 M BICINE PH=9.1 24% PEG 10K, pH 9.10 |