2BXW
CRYSTAL STRUCTURE OF RHOGDI Lys(135,138,141)Tyr MUTANT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR591 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2005-06-03 |
Detector | RIGAKU RAXIS IV |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 77.308, 77.308, 171.659 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 66.960 - 2.400 |
R-factor | 0.18 |
Rwork | 0.178 |
R-free | 0.22200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1kmt |
RMSD bond length | 0.008 |
RMSD bond angle | 2.264 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.090 | 0.180 |
Number of reflections | 23248 | |
<I/σ(I)> | 26.1 | 6.44 |
Completeness [%] | 97.1 | 80.8 |
Redundancy | 7.9 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.88 | 4M NA FORMATE, pH 7.88 |