2BWL
Murine angiogenin, phosphate complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2000-08-09 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 63.619, 56.672, 35.690 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.330 - 1.620 |
R-factor | 0.177 |
Rwork | 0.175 |
R-free | 0.20700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1agi |
RMSD bond length | 0.019 |
RMSD bond angle | 1.640 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.070 | 0.420 |
Number of reflections | 16648 | |
<I/σ(I)> | 16 | 4 |
Completeness [%] | 94.1 | 61.4 |
Redundancy | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.2 | 25% PEG 4000, 0.1M SODIUM PHOSPHATE BUFFER, PH 5.2 |