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2BDW

Crystal Structure of the Auto-Inhibited Kinase Domain of Calcium/Calmodulin Activated Kinase II

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.2
Synchrotron siteALS
Beamline8.2.2
Temperature [K]293
Detector technologyCCD
Collection date2004-12-18
DetectorADSC QUANTUM 4
Wavelength(s)0.9537
Spacegroup nameP 1 21 1
Unit cell lengths46.121, 77.104, 119.520
Unit cell angles90.00, 96.74, 90.00
Refinement procedure
Resolution45.800 - 1.800
R-factor0.216
Rwork0.216
R-free0.23600
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2phk
RMSD bond length0.008
RMSD bond angle1.200
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwareCNS (1.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]45.8001.910
High resolution limit [Å]1.8001.800
Number of reflections73357
Completeness [%]99.483.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION72931.6 M sodium malonate, 1.5 % 1,2,3-heptanetriol, pH 7.0, VAPOR DIFFUSION, temperature 293K

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