2BBQ
STRUCTURAL BASIS FOR RECOGNITION OF POLYGLUTAMYL FOLATES BY THYMIDYLATE SYNTHASE
Experimental procedure
Spacegroup name | P 63 |
Unit cell lengths | 127.100, 127.100, 67.900 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 * - 2.300 |
R-factor | 0.182 |
Rwork | 0.182 |
RMSD bond length | 0.015 |
RMSD bond angle | 3.300 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 9999.000 * |
High resolution limit [Å] | 2.240 * |
Rmerge | 0.091 * |
Total number of observations | 62321 * |
Number of reflections | 26307 * |
Completeness [%] | 86.8 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein solution | ||
2 | 1 | reservoir | potassium phosphate | 20 (mM) | |
3 | 1 | reservoir | ammonium sulfate | 2.3 (M) | |
4 | 1 | reservoir | DTT | 10 (mM) |