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2B52

Human cyclin dependent kinase 2 (CDK2) complexed with DPH-042562

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 5ID-B
Synchrotron siteAPS
Beamline5ID-B
Temperature [K]100
Detector technologyCCD
Collection date2000-12-15
DetectorMAR CCD 165 mm
Spacegroup nameP 21 21 21
Unit cell lengths72.030, 72.010, 53.500
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution18.710 - 1.880
Rwork0.219
R-free0.27500
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle1.700
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareEPMR
Refinement softwareCNX (2002)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0001.950
High resolution limit [Å]1.8801.880
Rmerge0.0660.747
Number of reflections23208
<I/σ(I)>21.13
Completeness [%]100.0100
Redundancy7.26.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.4291100mM HEPES pH 7.4, 50mM Ammonium Acetate, 2mM DTT, 4-14% PEG 4000 , VAPOR DIFFUSION, SITTING DROP, temperature 291K

217705

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