2ATI
Glycogen Phosphorylase Inhibitors
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Spacegroup name | P 31 |
Unit cell lengths | 124.500, 124.500, 123.200 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | ? - 1.900 |
R-factor | 0.234 |
Rwork | 0.232 |
R-free | 0.25600 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | MOSFLM |
Data scaling software | XDS |
Phasing software | AMoRE |
Refinement software | CNX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 500.000 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 167664 | |
Completeness [%] | 99.6 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |