Experimental procedure
| Temperature [K] | 293 |
| Detector technology | AREA DETECTOR |
| Collection date | 1992-04-14 |
| Detector | SIEMENS |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 82.600, 60.000, 66.200 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 6.000 - 2.480 |
| R-factor | 0.19 * |
| Rwork | 0.190 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 2.100 |
| Data reduction software | XENGEN |
| Phasing software | X-PLOR |
| Refinement software | TNT |
Data quality characteristics
| Overall | |
| Rmerge | 0.083 |
| Number of reflections | 10591 |
| Completeness [%] | 92.0 |
| Redundancy | 0.98 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 6.4 * | 293 * | pH 6.2 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | ammonium salfate | 20 (%) | |
| 2 | 1 | drop | PIPES | 10 (mM) | |
| 3 | 1 | drop | 2-mercaptoethanol | 2 (mM) | |
| 4 | 1 | drop | beta-octylglucoside | 20 (mM) | |
| 5 | 1 | reservoir | ammonium sulfate | 35 (%) | |
| 6 | 1 | reservoir | PIPES | 50 (mM) | |
| 7 | 1 | reservoir | 2-mercaptoethanol | 2 (mM) | |
| 8 | 1 | reservoir | beta-octylglucoside | 20 (mM) |
