2AG5
Crystal Structure of Human DHRS6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2005-07-14 |
Detector | RIGAKU RAXIS |
Spacegroup name | P 1 |
Unit cell lengths | 62.092, 62.055, 74.042 |
Unit cell angles | 106.05, 105.95, 100.97 |
Refinement procedure
Resolution | 66.670 - 1.840 |
R-factor | 0.16797 |
Rwork | 0.167 |
R-free | 0.22417 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.022 |
RMSD bond angle | 1.744 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.670 | 1.900 |
High resolution limit [Å] | 1.840 | 1.840 |
Number of reflections | 76176 | |
Completeness [%] | 89.7 | 52.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298 | Ammonium sulphate, Mes, PEG monomethylether 5000, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 298.0K |