2ZUQ
Crystal structure of DsbB-Fab complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-05-19 |
Detector | MACSCIENCE |
Wavelength(s) | 0.90 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 269.307, 51.480, 125.845 |
Unit cell angles | 90.00, 106.89, 90.00 |
Refinement procedure
Resolution | 45.640 - 3.300 |
R-factor | 0.27949 |
Rwork | 0.275 |
R-free | 0.35119 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1igt |
RMSD bond length | 0.011 |
RMSD bond angle | 1.492 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0044) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.510 | 3.480 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.086 | 0.865 |
Number of reflections | 25296 | |
<I/σ(I)> | 11.7 | 1.7 |
Completeness [%] | 99.5 | 97 |
Redundancy | 3.7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 293 | 15% PEG3350, pH 7, VAPOR DIFFUSION, temperature 293K |