Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.1 |
| Synchrotron site | BESSY |
| Beamline | 14.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-01-21 |
| Detector | RAYONIX |
| Spacegroup name | P 1 |
| Unit cell lengths | 37.920, 53.680, 58.109 |
| Unit cell angles | 100.27, 90.93, 94.19 |
Refinement procedure
| Resolution | 42.760 - 1.900 |
| R-factor | 0.18358 |
| Rwork | 0.181 |
| R-free | 0.23112 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2VRV |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.582 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.970 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.120 | 0.370 |
| Number of reflections | 36185 | |
| <I/σ(I)> | 8.8 | 2.16 |
| Completeness [%] | 94.0 | 84.4 |
| Redundancy | 2.9 | 2.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 25% PEG 3350, 0.1M HEPES PH 7.0, 0.2M NACL |
