2X6T
AGME bound to ADP-B-mannose
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARMOSAIC 225 mm CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 341.993, 60.787, 191.789 |
| Unit cell angles | 90.00, 91.41, 90.00 |
Refinement procedure
| Resolution | 38.690 - 2.360 |
| R-factor | 0.19032 |
| Rwork | 0.189 |
| R-free | 0.20889 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1eq2 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.956 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.4.0067) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.390 |
| High resolution limit [Å] | 2.350 | 2.350 |
| Rmerge | 0.040 | 0.190 |
| Number of reflections | 162824 | |
| <I/σ(I)> | 27 | 1.9 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 1.9 | 1.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
