2WTY
Crystal structure of the homodimeric MafB in complex with the T-MARE binding site
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARRESEARCH |
| Spacegroup name | P 2 21 21 |
| Unit cell lengths | 41.150, 49.820, 170.370 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 170.370 - 2.900 |
| R-factor | 0.237 |
| Rwork | 0.235 |
| R-free | 0.27500 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.258 |
| Refinement software | REFMAC (5.5.0044) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 19.000 |
| High resolution limit [Å] | 2.900 |
| Rmerge | 0.100 |
| Number of reflections | 8174 |
| <I/σ(I)> | 6.8 |
| Completeness [%] | 100.0 |
| Redundancy | 6.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
