Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2006-08-28 |
| Detector | RIGAKU IMAGE PLATE |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 63.630, 132.713, 161.287 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 102.600 - 2.300 |
| R-factor | 0.18315 |
| Rwork | 0.181 |
| R-free | 0.22715 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1bzl |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.956 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.5.0082) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.070 | 2.420 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.050 | 0.100 |
| Number of reflections | 55415 | |
| <I/σ(I)> | 22.9 | 9.2 |
| Completeness [%] | 94.9 | 85.7 |
| Redundancy | 5 | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8 | 0.1 M BIS-TRIS PH 8.0, 2.0 AMMONIUM SULFATE, 5 % PEG 400 |
