2VM9
Native structure of the recombinant discoidin II of Dictyostelium discoideum at 1.75 angstrom
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-08-23 |
Detector | ADSC CCD |
Spacegroup name | H 3 2 |
Unit cell lengths | 81.833, 81.833, 257.823 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.000 - 1.750 |
R-factor | 0.151 |
Rwork | 0.150 |
R-free | 0.17800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | MERCURY STRUCTURE |
RMSD bond length | 0.014 |
RMSD bond angle | 1.492 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.000 | 1.840 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.080 | 0.350 |
Number of reflections | 34043 | |
<I/σ(I)> | 7.5 | 2.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 10.9 | 11 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 200 MM AMMONIUM PHOSPHATE MONOBASIC, 100 MM TRIS PH 8.5, 50 % MPD |