2VL8
CRYSTAL STRUCTURE OF THE CATALYTIC DOMAIN OF LETHAL TOXIN FROM CLOSTRIDIUM SORDELLII IN COMPLEX WITH UDP, CASTANOSPERMINE AND CALCIUM ION
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 57.689, 191.332, 205.384 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 95.780 - 2.310 |
| R-factor | 0.218 |
| Rwork | 0.217 |
| R-free | 0.25500 |
| Structure solution method | OTHER |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.372 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 95.780 | |
| High resolution limit [Å] | 2.310 | 2.310 |
| Rmerge | 0.160 | 0.440 |
| Number of reflections | 100405 | |
| <I/σ(I)> | 11 | 5.2 |
| Completeness [%] | 99.6 | 98.9 |
| Redundancy | 8 | 8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
